| MS Description
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Sample metabolomic data were acquired usin … Sample metabolomic data were acquired using four time-of-flight mass spectrometers (TOF-MS), including CE-TOF-MS for analysis of polar metabolites, GC-TOF-MS for analysis of primary metabolites, LC-Q-TOF-MS for analysis of secondary metabolites and LC-IT-TOF-MS for analysis of lipids. Analysis was performed in triplicate, and the samples were extracted from each pipeline using optimized methods. <br />
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The experimental procedures for the GC‐, CE‐ and LC‐IT‐TOF‐MS pipelines were as reported previously (Kusano et al., 2007b; Okazaki et al., 2009; Oikawa et al., 2011). kazaki et al., 2009; Oikawa et al., 2011).
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